Simple Fabrication of Polycaprolactone-co-lactide Membrane with Silver Nanowires: Synthesis, Characterization and Cytotoxicity Studies 


Vol. 23,  No. 11, pp. 2983-2993, Nov.  2022
10.1007/s12221-022-4994-2


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  Abstract

Our simple technique of polymer/metal-based material preparation produces very promising material, and we outline that this material can be suitable for the potential wound healing multilayered dressing. In our research we focused on these main issues: (1) the preparation of silver nanowire-like structures using gallic acid (GA); (2) direct silver nanowire-like structure crystallization of co-polymer L-lactide and 琯-caprolactone (PLCL) electrospun fiber and (3) evaluation of the material cytotoxicity on the Vero cell line. Synthesized silver nanowire-like width varied from 30 to 100 nm and the hexagonal particles had sizes from 80 to 300 nm. The detected structures were crystalline cubic silver and were similarly synthesized during both batch synthesis and direct synthesis on the PLCL fibers. The amount of the silver spread within the fibrous membrane was approximately 1.1 wt. % in the sample, moreover, the silver incorporation had no influence on the polymer structure, which was confirmed by FTIR measurement. The cytotoxicity testing estimated that cell survival increased with decreased concentration of GA and silver in the PLCL matrix and the silver-based sample in 50 % MTT extraction concentration maintained required non-cytotoxic properties.

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  Cite this article

[IEEE Style]

Z. 힋imonov찼, L. Porubov찼, A. Verner, R. Gabor, Z. Vilamov찼, E. Dobro훾ka, M. Cieslar, V. Krbe훾kov찼, K. P. D휎dkov찼, L. Svoboda, J. Bedn찼힂, R. Dv, "Simple Fabrication of Polycaprolactone-co-lactide Membrane with Silver Nanowires: Synthesis, Characterization and Cytotoxicity Studies," Fibers and Polymers, vol. 23, no. 11, pp. 2983-2993, 2022. DOI: 10.1007/s12221-022-4994-2.

[ACM Style]

Zuzana 힋imonov찼, Ludmila Porubov찼, Adam Verner, Roman Gabor, Zuzana Vilamov찼, Edmund Dobro훾ka, Miroslav Cieslar, Veronika Krbe훾kov찼, Kate힂ina Peterek D휎dkov찼, Ladislav Svoboda, Ji힂챠 Bedn찼힂, and Richard Dv. 2022. Simple Fabrication of Polycaprolactone-co-lactide Membrane with Silver Nanowires: Synthesis, Characterization and Cytotoxicity Studies. Fibers and Polymers, 23, 11, (2022), 2983-2993. DOI: 10.1007/s12221-022-4994-2.

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pISSN : 1229 - 9197
eISSN : 1875 - 0052

Impact Factor(2022): 2.5