pISSN : 1229-9197 / eISSN : 1875-0052
Fibers and Polymers, the journal of the Korean Fiber Society, provides you with state-of-the-art
research in fibers and polymer science and technology related to developments in the textile
industry. Bridging the gap between fiber science and polymer science, the journal’s topics
include fiber structure and property, dyeing and finishing, textile processing, and apparel science.
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Latest Publication (Vol. 26, No. 7, Jul. 2025)
Composite Thermoplastic Polyurethane Nanofiber Membrane in Waterproof and Breathable Application
Xianmiao Pan Hongjie Wang Jiani Wang He Wang Hu Shi Shubo Wang Fangtao Ruan Quan Feng
Thermoplastic polyurethane (TPU) electrospun membrane is an ideal substrate material, especially in waterproof breathable membranes due to its superior mechanical properties and flexibility. Herein, we fabricate a TPU-based composite membrane by decorating ground polyacrylonitrile (PAN)-derived carbon nanofibers (CNFs) through ultrasonication followed by a dip-coating of polydimethylsiloxane (PDMS). The decorated CNFs can build up roughness on the membrane, and the coated PDMS layer can protect the CNFs from detaching from the membrane and increase the mechanical properties of the composite membrane. The obtained TPU/CNFs/PDMS membrane displays excellent waterproof and breathable ability. Specifically, the air permeability of the composite membrane is 7.38 mm/s, and the moisture permeability amounted to 5610 g/m2/day. Besides, the TPU/CNFs/PDMS membrane exhibited an outstanding tensile strength of 19.407 MPa, elongating at a break of 155.76%. This novel TPU-based composite membrane exhibits great application potential in functional fabric, especially for personal protective fabrics.
One-Pot Fabrication of Durable Conductive Cotton Fabrics Using Silver Composite Coating-Based DNA as a Template
Qingbo Xu Jinlong Zhang Fusheng Yang Yong Wang
Conductive cotton fabrics have important applications in the fields of flexible sensors and intelligent wearables. However, the low durability and complex preparation processes of conductive cotton fabrics limit their applications. In this study, a durable conductive cotton fabric was successfully prepared using a one-pot method. First, a stable colloidal solution containing deoxyribonucleic acid (DNA) segments, carboxymethyl chitosan (CMCTS), and Ag nanoparticles was prepared (DNA/CS/Ag). Thereafter, the prepared DNA/CS/Ag colloidal solution was applied to the fabric sample via one-pot strategy. The cotton fabric obtained demonstrated outstanding electrical conductivity and remarkable durability. The surface resistance of the fabricated sample was determined as 13.1 ± 0.7 Ω/sq. Additionally, even after the fabricated fabric endured 800 bending instances, 100 folding rounds, or stretching actions, the surface resistance of the sample showed no substantial decline. Furthermore, the characteristic features of the sample did not obviously change. Consequently, the conductive cotton fabric developed through the one-pot method holds great promise for applications in both the apparel sector and industrial domains.
Development of Cotton Fabric Loaded with Ag@ZnONPs as a Promising Reusable Antimicrobial Microfilter for Degrading the Methylene Blue Dye from Highly Polluted Water
Hany M. Abd El-Lateef Mohamed Gouda Manal F. Abou Taleb Mahmoud A. Abdelaziz Mai. M. Khalaf
The present study aimed to develop an environmentally friendly cotton fabric (CF) loaded with silver-doped zinc oxide nanoparticles (Ag@ZnONPs) as a microfilter for degrading methylene blue (MB) dye under visible light and prohibiting the growth of pathogenic bacteria presented in the contaminated water. The Ag@ZnONPs were prepared using precipitation and doping methods. The precipitation method was used for ZnONPs preparation, then the doping method for the deposition of AgNPs onto the surface of the prepared ZnONPs. After preparation, a small concentration was used to functionalize CF. Ag@ZnONPs were characterized using TEM and DLS analysis, illustrating the formation of nanoparticles with nearly spherical small size (55.91 nm) and PdI (0.630). Ag@ZnONPs-loaded CF exhibited a rough surface owing to the deposition of nanoparticles on the CF surface. Meanwhile, the untreated CF exhibited a smooth surface. The results showed that the Ag@ZnONPs-loaded CF exhibited excellent photocatalytic degradation of MB dye molecules under visible light, with degradation efficiencies reaching 100% within 150–180 min of irradiation. Moreover, the filter demonstrated significant antibacterial activity against the tested pathogenic bacteria, forming inhibition zones with diameters ranging from 15 ± 0.62 to 19 ± 0.56 mm. The biocompatibility and toxicity of the Ag@ZnONPs-loaded CF were also assessed, showing no significant toxicity issues and indicating its safe use in environmental applications. In addition, SEM analysis revealed the destructive effects of Ag@ZnONPs on the bacterial cells, further supporting its antibacterial efficacy. Overall, Ag@ZnONPs-loaded CF filter has shown great promise as a microfilter for the simultaneous removal of contaminants, degradation of organic dyes, and killing of pathogenic microbes from contaminated water, offering a sustainable and cost-effective solution for water purification.
Study and Development of Natural Antibacterial Finished Milkweed and Milkweed/Recycled Hollow Polyester Blended Textile Materials using Senna Auriculata Component for Feminine Health and Hygiene Products
Rajesh kumar C Raja D
Menstrual hygiene management remains a significant challenge, emphasizing the need for hygienic, moisture-managing, and antibacterial sanitary materials. Conventional sanitary napkins predominantly use synthetic materials in their layers, which can cause discomfort and health issues for users, particularly due to bacterial growth in menstrual blood. This study addresses these concerns by developing a natural antibacterial textile material using Senna auriculata flower, known for its antibacterial and antifungal properties. Powdered components of Senna auriculata were applied to milkweed and milkweed/recycled hollow polyester blended nonwoven textile material through extracted component finishing and nanoparticle finishing techniques. The developed sanitary napkin design incorporated polypropylene nonwoven as the top layer, antibacterial finished milkweed and recycled hollow polyester textile material as antibacterial textile layer between the top and core layers to inhibit bacterial proliferation, recycled viscose fiber as the core absorbent, and polyethylene as the bottom barrier layer. The performance of the treated materials was evaluated against Staphylococcus aureus, Klebsiella pneumoniae, and Escherichia coli, demonstrating significant antibacterial efficacy. Moisture behavior properties, including liquid spreading rate, retention capacity, holding capacity under pressure, and absorption capacity, were analyzed. The results confirmed improved antibacterial functionality and enhanced moisture management, providing an enhanced and effective solution for menstrual hygiene products and management. This study offers a safer, more comfortable, and eco-friendly solution for menstrual hygiene products.
In Situ Synthesis of Cuprous Oxide with Honeysuckle Extract for Developing Durable Antimicrobial Cotton Fabric
Yonggang Peng Zhou Fang Suyu Pan Ziyong Lu Shiping Luo
The immobilization of nanoparticles (NPs) onto cotton fiber (CF) is a promising method for preparing antimicrobial textile, but NPs on the CF surface will leach out after several washing cycles, which leads to the deterioration of antimicrobial property and environmental pollution. Herein, to facilitate the penetration of Cu2+ ions into the interior of fibers, the treatment of CF using NaOH solution mixed with Cu2+ was proposed. Furthermore, hydrophobic and antimicrobial CF was prepared by in situ reduction of Cu2+ to cuprous oxide (Cu2O) using honeysuckle (Lonicera japonica Thunb) extract, followed by immersion in stearic acid (SA) ethanol solution. Even if the initial Cu2+ concentration was as low as 0.008 mol/L, the antimicrobial rates of the prepared hydrophobic Cu2O-cotton fabric (Cu2O-CF@SA) against Escherichia coli (E. coli), Staphylococcus aureus (S. aureus), and Candida albicans (C. albicans) were as high as 99.99%. Moreover, the prepared Cu2O-CF@SA also displayed excellent mechanical robustness and laundering durability, maintaining over 92% antimicrobial activity against E. coli and S. aureus after 50 tap-peeling cycles or 20 laundering cycles. The outstanding property of Cu2O-CF@SA offers great potentiality in antimicrobial fabric applications such as medical textiles (surgical gowns/masks), wound dressings, sportswear, and so on. This work provides an innovative method for the preparation of Cu2O using honeysuckle extract as green reductant for developing CF with durable antimicrobial activity.
Cotton Fabric Coated with Ag/ZnO/SiO2 for Methyl Orange Degradation and Bacterial Suppression in Water Treatment
Mohamed Gouda Mai M. Khalaf Manal F. Abou Taleb Mahmoud A. Abdelaziz Hany M. Abd El-Lateef
The present study aimed to develop a multifunctional cotton fabric filter capable of eliminating pathogenic microbes and degrading the organic dyes in polluted wastewater. To achieve this aim, bleached plain weaved cellulosic fabric (BPWCF) was treated by immersion in the nanocomposite solution of Ag/ZnO/SiO2 and then dried and cured for fixation of nanocomposites onto the surface of BPWCF. Initially, Ag/ZnO/SiO2 nanocomposite was prepared from silica, zinc, and Ag salts, namely, tetraethyl orthosilicate, zinc nitrate, and silver nitrate, respectively. The results indicated that nanocomposite was prepared (168 nm, PdI value 0.284). After the success of the nanocomposite preparation, it was used for BPWCF treatment to produce efficient multifunctional BPWCF (Ag/ZnO/SiO2 nanocomposite-loaded BPWCF). The results indicate that methyl orange (MO) could be removed entirely in 120 min of reaction time using the Ag/ZnO/SiO2 nanocomposite as a catalyst in conjunction with BPWCF to efficiently increase the photocatalytic degradation of MO. Regarding the tested materials’ antibacterial properties, results showed that such promising filter had a vigorous antibacterial action against Gram-positive and Gram-negative bacteria. In conclusion, these findings demonstrate that the Ag/ZnO/SiO2 nanocomposite-loaded BPWCF exhibits excellent multifunctionality, effectively promoting the photocatalytic degradation of wastewater dyes and the inactivation of pathogenic microbes, highlighting its strong potential for application in environmental remediation.
Fabrication of Biomass-Based Flame-Retardant Fabrics via Foam Finishing with Co-efficiency of Phytic Acid and Zinc Ions
Xiaokai Xin Rong Guo Peibo Du Jinyun Wu Lei Zhang Weizhong Zhang Fengyan Ge
Cotton fabrics are extensively used for their comfort and biodegradability. However, their flammability presents a significant fire risk, necessitating the urgent enhancement of their flame-retardant properties. Phytic acid, a natural compound with high phosphorus content, offers potential as a flame retardant but has limited efficacy. The incorporation of metal ions, such as zinc, can synergistically enhance its performance. Foam finishing is a low-fluid, energy-efficient process that demonstrates significant advantages over conventional finishing techniques in terms of resource utilization and performance efficiency. This work developed highly flame-retardant cotton textiles using a green, low-additive liquid foam finishing technique by combining phytic acid and zinc acetate. The synergy between phytic acid and zinc ions significantly enhanced charring ability and flame-retardant performance of the fabric, achieving a limiting oxygen index (LOI) of 32.5% and reducing the char length to 4.3 cm. It is particularly noteworthy that this method utilizes biomass materials as both the flame-retardant finishing agent and the foaming agent, without the use of organic solvents or hazardous chemicals throughout the process. While achieving excellent flame-retardant performance, it effectively preserves the softness and comfort of the fabric, thereby combining environmental friendliness with high application efficiency. This study integrates foam finishing with biomass-based flame retardancy, proposing a simple, eco-friendly method aligned with sustainable development principles, and demonstrating strong potential for large-scale production of flame-retardant cotton fabrics.
Synthesis of a Dopo-Based Imidazole Compound and Analysis of its Flame Retardant Pet Fabric
Xin Yan Yong Shen Hong Pan Yihong Wang Lihui Xu Liming Wang
Polyester (PET) textiles, which are widely used in interior furnishings, seating and clothing, are highly flammable and readily produce high temperature melt droplets, which present significant safety hazards in everyday use. To enhance the flame retardant and anti-melt drop properties of PET fabrics, the DOPO derivative (DTA) with benzimidazole structure was synthesised. Furthermore, the silica sol was prepared with the silane coupling agent KH602, which was used as an additive. When the total loading was 15% and the mass ratio of DTA to KH602 was 2:1, the LOI value of the flame-retardant PET fabric was 29.2%, and the melt drop was completely inhibited. In addition, the HRC and PHRR were reduced by 54% and 68%, respectively, compared to the untreated fabric. The thermogravimetric tests showed that the carbon content of the flame retarded PET fabric increased from 6.5 to 20.7% in the higher temperature zone. Scanning electron microscopy of the residual char showed that the flame retardant facilitated the formation of the expansive char layer on the PET fabric. The mechanism of the DTA/KH602 flame retarded PET fabric was investigated based on the results of thermal cracking gas chromatography, Raman spectroscopy, and X-ray photoelectron spectroscopy of the residual char. The results showed that DTA/KH602 exerted a flame retardant effect in both the gaseous and condensed phases. The expanded carbon layer, which is rich in phosphorus and silicon elements, acts as a support structure and inhibits the dripping of molten droplets.
Chemical Modification of Polyester Knitted Fabric with Ultrasound to Improve Hydrophilicity and Wettability
Marija Kodrić Dragan Đorđević Anita Tarbuk Shahidul Islam Ivana Čorak Suzana Đorđević K. Z. M. Abdul Motaleb
The study introduces a novel and innovative pretreatment or surface modification method for polyester fibers that enhances their hydrophilicity and moisture sorption. The modification alters the surface morphology of the fibers, resulting in reduced mass and improved sorption properties. The objective is to make the surface of polyester fibers more accessible to various agents, such as water, dyes, and finishing chemicals. The modification of polyester knitted fabric is performed in alcoholic and alkali-alcoholic solutions using ultrasound. The mass loss after modification ranges from 3.6 to 8.5%, depending on the type of treatment. The isoelectric point values for both unmodified and modified samples range from pH 2.5 to pH 3.1. During the process, the samples exhibit varying negative surface charges: KOH-Octanol treatment, pH 5, ζ = - 30 mV; octanol treatment, pH 5, ζ = - 20 mV; unmodified sample, pH 5, ζ = - 15 mV. The research results demonstrate that water absorption, capillarity, and wetting time are significantly improved in all cases for the modified polyester samples. The drop in burst resistance reaches a maximum of 12%. The contribution of this study lies in the application of novel agents for polyester modification and innovative processing procedures, which together enhance the properties and functionality of polyester fibers in a simple and effective manner.
Polyhexamethylene Guanidine-Treated Cotton Fabric as Self-Decontaminating Materials for Advanced Protective Clothing Against Nerve Agents
Woong Kwon Euigyung Jeong
Fabrics treated with organic catalysts containing guanidine groups have shown promise as protective materials against nerve agents. This study proposes a simple method for incorporating guanidine groups onto cotton fabric surfaces using polyhexamethylene guanidine (PHMG) to develop protective materials against nerve agents. The detoxification performance of the prepared fabric was assessed using nerve agent simulants, including dimethyl methylphosphonate (DMMP) and diisopropylfluorophosphate (DFP). PHMG-treated cotton fabric decontaminated 27.6% of DMMP and 67.2% of DFP at 32 °C in 2 h, with half lives of 401 and 229 min, respectively. These findings indicate that PHMG-treated cotton fabric exhibits strong detoxification performance against nerve agent simulants. Therefore, PHMG can be considered an effective organic catalyst for the simple and facile fabrication of protective materials against nerve agents.